HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Tetrachloride → 1-Chlorocyclohexanecarbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Tetrachloride | HCID 5943 | — |
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Cyclohexanecarbonyl chloride | HCID 75938 | — |
| Product | 1-Chlorocyclohexanecarbonyl chloride | HCID 12228222 | — |
Reaction Steps
80 g (0.547 mol) of cyclohexanecarboxylic acid chloride, 30 ml of carbon tetrachloride, 63 ml (0.778 mol) of SO2Cl2 and 1.5 g of benzoyl peroxide are heated for 10 hours. The chlorinated acid chloride is then distilled from the reaction mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954730 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-bc7d72b648544d949e455066e81eeec9 |
| Source note | uspto-grants-1976_05 |