HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 5-Fluorouracil
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 12610212 | HCID 12610212 | — |
| Product | 5-Fluorouracil | HCID 3385 | 49.9% |
Reaction Steps
0.25 g of 5-fluoro-6-methoxy-5,6-dihydrouracil obtained in Example 1B above was placed in a reflux flask and then 1 ml of concentrated HCl was added to the flask. The flask contents were brought to refluxing temperature, and the precipitation of a solid soon occurred, producing 0.1 g of 5-fluorouracil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954759 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-350f13e7133944a0898dd29a0ffca105 |
| Source note | uspto-grants-1976_05 |