HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzoyl chloride → HCID 20441568, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzoyl chloride | HCID 70276 | — |
| Reactant | HCID 86733381 | HCID 86733381 | — |
| Solvent | Diethyl ether ethanol | HCID 21585056 | — |
| Product | HCID 20441568 | HCID 20441568 | — |
Reaction Steps
Produced in a manner analogous to that described in Example 8 (g), from 28.5 g of 3-chloro-5,6,7,8-tetrahydropyrido[4,3-c]pyridazine maleate and 16.9 g of o-toluoyl chloride. Reaction time 24 hours. M.P. 123°-126° (decomp., from 95% ethanol/ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954754 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-08ade4c2937a4148a130308c9888bcbe |
| Source note | uspto-grants-1976_05 |