HRID1075960

反应详情

EQUATION

反应方程式

HRID 1075960 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 0.300 g. of 2-hydroxyethylhydrazine and 0.4 g. of 1-methyl-2-nitro-5-imidazolecarboxaldehyde in 20 ml. of methanol is allowed to stand for two days. The solid which precipitates is recovered on the filter and washed with water. Yield: 0.245 g., m.p. 138°-140° C.

WORKUP

后处理

  1. customThe solid which precipitates
  2. customis recovered on the
  3. filtrationfilter
  4. washwashed with water