HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 21541502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Hydrogen Cyanide | HCID 768 | — |
| Reactant | Triethylaluminum | HCID 16682930 | — |
| Reactant | HCID 21541489 | HCID 21541489 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 21541502 | HCID 21541502 | 44.4% |
Reaction Steps
The procedure similar to that of Step 3 (a) of Example 1 was repeated using 9.4 g of 2-(6'-carbethoxyhexyl)-3-methoxy-4-hydroxy- 2-cyclopenten-1-one, 8.2 g of triethyl aluminum, 2.0 g of hydrocyanic acid, and a mixed solvent of benzene and toluene to provide 4.1 g of oily 2-(6'-carbethoxyhexyl)-3-cyano-4-hydroxy-2-cyclopenten-1-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954811 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-203959e7dda84596a46156220ef412a8 |
| Source note | uspto-grants-1976_05 |