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HRID1076036

反应详情

EQUATION

反应方程式

HRID 1076036 的结构方程式

REACTANTS

反应物

4
结构：CO
HCID887

Methanol

CH4O

结构：CC(C)(O)C#N
HCID6406

2-Hydroxy-2-methylpropanenitrile

C4H7NO

结构：O=C([O-])[O-].[Na+].[Na+]
HCID10340

Carbonic acid sodium salt (1:2)

CNa2O3

结构：CCCCCCC1=CCCC1=O
HCID66768

2-Hexylcyclopent-2-enone

C11H18O

PRODUCTS

生成物

1
结构：CCCCCCC1C(=O)CCC1C#N
HCID11298483

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

A mixture of 16,6 g of 2-n-hexyl-2-cyclopentenone (see foot note (1) under Table II) 12 g of acetone cyanhydrine (Org.Synth.Coll. Vol. 2, p. 7), 32 ml of methanol and 0,8 g of sodium carbonate in 12 ml of water, is heated at reflux temperature for 31/2 hours.

WORKUP

后处理

  1. temperatureis heated
  2. temperatureat reflux temperature for 31/2 hours