HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 2-n-Hexyl-3-cyanocyclopentanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Acetone Cyanohydrin | HCID 6406 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 2-Hexyl-2-cyclopenten-1-one | HCID 66768 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-n-Hexyl-3-cyanocyclopentanone | HCID 11298483 | — |
Reaction Steps
A mixture of 16,6 g of 2-n-hexyl-2-cyclopentenone (see foot note (1) under Table II) 12 g of acetone cyanhydrine (Org.Synth.Coll. Vol. 2, p. 7), 32 ml of methanol and 0,8 g of sodium carbonate in 12 ml of water, is heated at reflux temperature for 31/2 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954834 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-cd41f07a5efb4572a6d84d32084f7888 |
| Source note | uspto-grants-1976_05 |