Benzyl Bromide → HCID 53689962, compound

HRID 1076064Notes

Reaction equation

HRID 1076064 reaction equation
BrBr.[F:3][C:4]1[CH:10]=[C:8]([NH2:9])[C:7]([CH3:11])=[CH:6][CH:5]=1.C([Br:19])C1C=CC=CC=1>>[F:3][C:4]1[CH:10]=[C:8]([NH:9][Br:19])[C:7]([CH3:11])=[CH:6][CH:5]=1

Participants

4

Reactant 3

HCID 7498Benzyl BromideHCID 24408BromineHCID 677745-Fluoro-o-toluidine

Product 1

HCID 53689962HCID 53689962, compound

Procedure

Bromine (0.5 mole) is added over 1 hour to stirred 5-fluoro-o-toluidine (0.5 mole) at 100° C illuminated with a high wattage lamp. The crude benzyl bromide is used as prepared.

Workup

  1. customilluminated with a high wattage lamp
  2. customas prepared

Sources & evidence

ORD record
ord-2df1c17d8b8446ea9834e7a1c47c0ae8
Source dataset
uspto-grants-1976_05
Patent number
US03954852

Reaction notes

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