HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → HCID 68136348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | HCID 21541773 | HCID 21541773 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 68136348 | HCID 68136348 | — |
Reaction Steps
To 1.20 g of 1-(3-methyl-4-methylthiophenyl)-2-isopropylaminoethanol in 40 ml of ether, 0.45 g of oxalic acid in 50 ml of ether are dropwise added while stirring. The precipitate is filtered and washed with ether, then crystallised from a methanol-ether mixture. MP (°C): 165.5° - 167.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954871 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-d095d552bc6849c8bed7e3a65e3bf9b6 |
| Source note | uspto-grants-1976_05 |