Methyl p-toluenesulfonate → HCID 21541914, compound

HRID 1076110Notes

Reaction equation

HRID 1076110 reaction equation
[CH3:1][N:2]([CH2:6][CH2:7][OH:8])[CH2:3][CH2:4][OH:5].[C:9]1([CH3:20])[CH:14]=[CH:13][C:12]([S:15]([O:18]C)(=[O:17])=[O:16])=[CH:11][CH:10]=1>>[C:9]1([CH3:20])[CH:10]=[CH:11][C:12]([S:15]([O-:18])(=[O:16])=[O:17])=[CH:13][CH:14]=1.[CH3:1][N+:2]([CH3:9])([CH2:6][CH2:7][OH:8])[CH2:3][CH2:4][OH:5]

Participants

3

Reactant 2

HCID 6645Methyl p-toluenesulfonateHCID 7767N-Methyldiethanolamine

Product 1

HCID 21541914HCID 21541914, compound

Procedure

Dimethyl di (βhydroxyethyl) ammonium para-toluene sulfonate (A) is prepared from methyl diethanolamine being added slowly and with stirring to methyl para-toluene sulfonate. Product (A) is rinsed and dried under slightly lowered pressure.

Workup

  1. additionadded slowly
  2. washProduct (A) is rinsed
  3. customdried under slightly lowered pressure

Sources & evidence

ORD record
ord-f5b35b6fc2a041758ce3c4c63bf003e0
Source dataset
uspto-grants-1976_05
Patent number
US03954902

Reaction notes

Loading…