Sorbitol → HCID 131710197, compound

HRID 1076150Notes

Reaction equation

HRID 1076150 reaction equation
[CH:1](=[C:8]([C@@H:10]([C@H:12]([C@@H:14]([C@@H:16]([CH2:18][OH:19])[OH:17])[OH:15])[OH:13])[OH:11])[OH:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.O[CH2:21][C@@H]([C@H]([C@@H]([C@@H](CO)O)O)O)O.C1(C)C=CC(C=O)=CC=1>C1CCCCC1>[CH3:21][C@:10]([C@H:12]([C@@H:14]([C@@H:16]([CH2:18][OH:19])[OH:17])[OH:15])[OH:13])([OH:11])[C:8](=[CH:1][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1)[OH:9]

Participants

5

Reactant 3

HCID 5780Sorbitol2×HCID 77254-Methylbenzaldehyde2×HCID 66689111HCID 66689111, compound

Product 1

HCID 131710197HCID 131710197, compound

Reagents, catalysts & solvents 1

HCID 8078CyclohexaneSolvent

Procedure

The methyl benzylidene sorbitol was prepared in like manner as the benzylidene sorbitol in the foregoing Example 1. in which 32.0 g of 70% sorbitol, 44.3 g of para-tolualdehyde and 580 ml of cyclohexane were used. The acetal value of the reaction product in white powder from was about 345 which corresponds to the combination ratio of 3.0 moles of paratolualdehyde per 1 mole of sorbitol.

Sources & evidence

ORD record
ord-517ef710c8114736b41c8723f7dc26cd
Source dataset
uspto-grants-1976_05
Patent number
US03955997

Reaction notes

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