Aminoacetaldehyde dimethyl acetal → HCID 178495877, compound

HRID 1076210Notes

Reaction equation

HRID 1076210 reaction equation
CO[C:3]1[CH:4]=[CH:5][C:6]2[C:12](=S)[NH:11][C:10]3[CH:14]=[CH:15][CH:16]=[CH:17][C:9]=3[NH:8][C:7]=2[CH:18]=1.[CH3:19][O:20][CH:21]([O:24][CH3:25])[CH2:22][NH2:23]>C(O)CCC>[CH3:19][O:20][CH:21]([O:24][CH3:25])[CH2:22][NH:23][C:12]1[C:6]2[CH:5]=[CH:4][CH:3]=[CH:18][C:7]=2[NH:8][C:9]2[CH:17]=[CH:16][CH:15]=[CH:14][C:10]=2[N:11]=1

Participants

4

Reactant 2

HCID 89728Aminoacetaldehyde dimethyl acetalHCID 21539202HCID 21539202, compound

Product 1

HCID 178495877HCID 178495877, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Procedure

In the manner given in Example 4, 3-methoxy-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepine-11-thione is treated with amino acetaldehyde dimethyl acetal in n-butanol to give [(5H-dibenzo[b,e][1,4]diazepin-11-yl)amino]acetaldehyde dimethyl acetal.

Sources & evidence

ORD record
ord-e986a7d7b06649fda70db1217835426e
Source dataset
uspto-grants-1976_05
Patent number
US03956297

Reaction notes

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