Carbon Dioxide → HCID 14417405, compound

HRID 1076234Notes

Reaction equation

HRID 1076234 reaction equation
C([CH:4]1[CH:8]([C:9]2[CH:14]=[CH:13][C:12]([Cl:15])=[CH:11][CH:10]=2)[CH:7]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[NH:6][C:5]1=[O:22])(O)=O.C1(C)C(C)=CC=CC=1.C(=O)=O>CCCCCC>[Cl:15][C:12]1[CH:13]=[CH:14][C:9]([CH:8]2[CH:7]([C:16]3[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=3)[NH:6][C:5](=[O:22])[CH2:4]2)=[CH:10][CH:11]=1

Participants

5

Reactant 3

HCID 280Carbon DioxideHCID 7237O-XyleneHCID 54403188HCID 54403188, compound

Product 1

HCID 14417405HCID 14417405, compound

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

12 g. of 3-carboxy-4-p-chlorophenyl-5-phenyl-2-pyrrolidinone in 200 ml. of xylene are refluxed until evolution of CO2 ceased (about 20 minutes). The solution is cooled, 200 ml. of hexane are added and the reaction product crystallizes out. 8 g. of 4-p-chlorophenyl-5-phenyl-2-pyrrolidinone are obtained. M.P. : 159°-160°C.

Workup

  1. custom(about 20 minutes)
  2. temperatureThe solution is cooled
  3. customthe reaction product crystallizes out

Sources & evidence

ORD record
ord-8c46f7db0ed84c928c20a29670ff5f7f
Source dataset
uspto-grants-1976_05
Patent number
US03956314

Reaction notes

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