HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 21486904, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Methyl 2-methoxy-2-(2-pyridyl)acetate | HCID 21486910 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21486904 | HCID 21486904 | — |
Reaction Steps
A mixture of 18.1 g. of methyl 2-methoxy-2-(2-pyridyl)acetate and 10 g. of dimethylamine in ethanol is stirred at room temperature for 26 hours. The mixture is concentrated, dissolved in chloroform and extracted with brine. The organic phase is dried over magnesium sulfate and filtered and the solvent is removed under reduced pressure to give 2-methoxy-N,N-dimethyl-2-(2-pyridyl)acetamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03956494 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-41df02ac05e54de2b054dd8c3f855d99 |
| Source note | uspto-grants-1976_05 |