HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-methoxy-N-methyl-3-morpholino-2-(2-pyridyl)thiopropanamide hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-methoxy-N-methyl-3-morpholino-2-(2-pyridyl)thiopropanamide | HCID 53846077 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-methoxy-N-methyl-3-morpholino-2-(2-pyridyl)thiopropanamide hydrochloride | HCID 86733196 | — |
Reaction Steps
One gram of 2-methoxy-N-methyl-3-morpholino-2-(2-pyridyl)thiopropanamide in ether is added to ethereal hydrogen chloride. The resulting precipitate is filtered off and recrystallized from ethanol/ether to give 2-methoxy-N-methyl-3-morpholino-2-(2-pyridyl)thiopropanamide hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03956494 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-5528fe86ee8040759f77d6552ca2b1b2 |
| Source note | uspto-grants-1976_05 |