HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → HCID 53996258, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 15581954 | HCID 15581954 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53996258 | HCID 53996258 | — |
Reaction Steps
A mixture of 19.5 g. of 2-dimethylamino-N-methyl-2-(2-pyridyl)thioacetamide in 200 ml. of methanol, 13 g. of morpholine and 4.5 g. of formaldehyde is heated at reflux for 48 hours. The mixture is concentrated in vacuo and the residue is recrystallized from isopropyl ether to give 2-dimethylamino-N-methyl-3-morpholino-2-(2-pyridyl)thiopropanamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03956494 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-85eb61bf96e8413f892992970db0eeb9 |
| Source note | uspto-grants-1976_05 |