HCID 131710229, compound → HCID 131710228, compound

Participants

Reaction Steps

858 mg of Z-Gly-Phe-Gly-Pro-Glu(OtBu)-Thr(tBu)-Pro-OtBu are hydrogenated in 150 ml of methanol in the presence of 200 mg of palladium-carbon catalyst (10% Pd). The product is triturated with ether×hexane (1:1) to form an amorphous powder. In the thin-layer chromatogram on silica gel it shows the following values:

Provenance & Evidence