HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Chloride → HCID 54240948, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Chloride | HCID 6327 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 131710231 | HCID 131710231 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 54240948 | HCID 54240948 | — |
Reaction Steps
The oxalate salt of example 1 is basified by treatment with K2CO3. A solution of the base in MeCN is cooled and treated with methyl chloride. The solution is allowed to stand for one day and the solvent is evaporated to give 3,3a,4,5,6,7-hexahydro-N,N-dimethyl-3-phenyl-7-(phenylmethylene)-2H-indazole-2-propanamine, methochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03957762 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-cfee91b4c2424430895317e4821f5edd |
| Source note | uspto-grants-1976_05 |