Hydrogen Peroxide → HCID 54240948, compound

HRID 1076501Notes

Reaction equation

HRID 1076501 reaction equation
C(O)(=O)C(O)=O.[CH3:7][N:8]([CH3:34])[CH2:9][CH2:10][CH2:11][N:12]1[CH:20]([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[CH:19]2[C:14]([C:15](=[CH:27][C:28]3[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=3)[CH2:16][CH2:17][CH2:18]2)=[N:13]1.OO>CO>[CH3:34][N:8]([CH3:7])[CH2:9][CH2:10][CH2:11][N:12]1[CH:20]([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[CH:19]2[C:14]([C:15](=[CH:27][C:28]3[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=3)[CH2:16][CH2:17][CH2:18]2)=[N:13]1

Participants

4

Reactant 2

HCID 784Hydrogen PeroxideHCID 131710231HCID 131710231, compound

Product 1

HCID 54240948HCID 54240948, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

A solution of the free base of example 1 in methanol is treated with two equivalents of 30% H2O2. The solution is allowed to stand for two days and the solvent is removed under reduced pressure to give 3,3a,4,5,6,7-hexahydro-N,N-dimethyl-3-phenyl-7-(phenylmethylene)-2H-indazole-2-propanamine, N-oxide.

Workup

  1. customthe solvent is removed under reduced pressure

Sources & evidence

ORD record
ord-fa81b9b0f9144a41b619f9a83d817d82
Source dataset
uspto-grants-1976_05
Patent number
US03957762

Reaction notes

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