Sodium Bicarbonate → HCID 21537282, compound

HRID 1076629Notes

Reaction equation

[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8](=[O:33])[C:9]1[CH:14]=[C:13]([Cl:15])[CH:12]=[CH:11][C:10]=1[N:16]1[CH:20]=[N:19][N:18]=[C:17]1[CH2:21][N:22]1[C:26](=[O:27])[C:25]2=[CH:28][CH:29]=[CH:30][CH:31]=[C:24]2[C:23]1=[O:32].[C:34](=[O:37])(O)[O-].[Na+]>>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8](=[O:33])[C:9]1[CH:14]=[C:13]([Cl:15])[CH:12]=[CH:11][C:10]=1[N:16]1[C:17]([CH2:21][N:22]2[C:23](=[O:32])[C:24]3=[CH:31][CH:30]=[CH:29][CH:28]=[C:25]3[C:26]2=[O:27])=[N:18][N:19]=[C:20]1[CH2:17][N:16]1[CH2:20][CH2:34][O:37][CH2:9][CH2:10]1

Participants

Reactant 2

HCID 516892Sodium Bicarbonate

HCID 21498873HCID 21498873, compound

Product 1

HCID 21537282HCID 21537282, compound

Procedure

In the manner given in Example 13, 2',5-dichloro-2-[3(phthalimidomethyl)-4H-1,2,4-triazol-4-yl]benzophenone is reacted with the above suspension then neutralized with sodium bicarbonate to give 2',5-dichloro-2-[3-(morpholinomethyl)-5-(phthalimidomethyl)-4H-1,2,4-triazol-4yl]-benzophenone.

Workup

customis reacted with the above suspension

Sources & evidence

ORD record: ord-f3b573a9302843b68f07906cc2a54ea7
Source dataset: uspto-grants-1976_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03957761

Reaction notes

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