HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131710241, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 12235832 | HCID 12235832 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 131710241 | HCID 131710241 | — |
Reaction Steps
To a solution of 1.0 g of 6H-pyrido [1,2-c][1,3,5]-benzoxadiazepine in 20 ml of 2-propanol is added 5.0 ml of 4.2N 2-propanolic hydrogen chloride. To the clear solution is added anhydrous ether until a turbidity forms. The pale yellow crystalline solid is filtered and recrystallized from acetonitrile to give about 1.0 g of the title compound, mp about 232°-234°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03957806 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-a17c4e21cd874a62b65d15ea37f1c7e2 |
| Source note | uspto-grants-1976_05 |