Hydrochloric Acid → HCID 12319472, compound

HRID 1076726Notes

Reaction equation

HRID 1076726 reaction equation
[Br:1][C:2]1[CH:15]=[CH:14][CH:13]=[CH:12][C:3]=1[CH:4]([OH:11])[C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1.Cl.[CH3:17]O>>[CH3:17][O:11][CH:4]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)[C:3]1[CH:12]=[CH:13][CH:14]=[CH:15][C:2]=1[Br:1]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 114255182-Bromo-α-phenylbenzenemethanol

Product 1

HCID 12319472HCID 12319472, compound

Procedure

A solution of 730 g. of 2-bromobenzhydrol and 25 l. of methanol is slowly heated to reflux over a 2 hour span while a stream of hydrogen chloride gas is bubbled into the solution. The solution is refluxed for 24 hours, and concentrated to a liquid. Distillation gives 2-bromobenzhydryl methyl ether as a pale yellow liquid, b.p. 125° - 128°C./0.2 mm.

Workup

  1. customis bubbled into the solution
  2. temperatureThe solution is refluxed for 24 hours
  3. concentrationconcentrated to a liquid
  4. distillationDistillation

Sources & evidence

ORD record
ord-02dabcecd78f4f8d804ea075eaf1b01a
Source dataset
uspto-grants-1976_05
Patent number
US03957828

Reaction notes

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