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HRID1076728

反应详情

EQUATION

反应方程式

HRID 1076728 的结构方程式

REACTANTS

反应物

2
结构：CN(C)CCCCl
HCID66960

Dimethylaminopropyl chloride

C5H12ClN

结构：c1ccc(C2OC3(CCOCC3)c3ccccc32)cc1
HCID12826085

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)CCCC1(c2ccccc2)OC2(CCOCC2)c2ccccc21.Cl
HCID12826087

未命名化合物

PROCEDURE

实验过程

By following the manipulative procedure described above in Example 1c, 3-dimethylaminopropyl chloride is reacted with 1,2',3,3',5',6'-hexahydro-3-phenylspiro(isobenzofuran-1,4'-pyran). The hydrochloride salt of the product is recrystallized from an acetone-ethyl ether mixture to give 3-(3-dimethylaminopropyl)-1,2',3,3',5',6'-hexahydro-3-phenylspiro[isobenzofuran-1,4'-pyran] hydrochloride, m.p. 234.5° - 235.5°C.

WORKUP

后处理

  1. customThe hydrochloride salt of the product is recrystallized from an acetone-ethyl ether mixture