HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-N,N-dimethyl-1-propanamine → HCID 12826087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-N,N-dimethyl-1-propanamine | HCID 66960 | — |
| Reactant | HCID 12826085 | HCID 12826085 | — |
| Product | HCID 12826087 | HCID 12826087 | — |
Reaction Steps
By following the manipulative procedure described above in Example 1c, 3-dimethylaminopropyl chloride is reacted with 1,2',3,3',5',6'-hexahydro-3-phenylspiro(isobenzofuran-1,4'-pyran). The hydrochloride salt of the product is recrystallized from an acetone-ethyl ether mixture to give 3-(3-dimethylaminopropyl)-1,2',3,3',5',6'-hexahydro-3-phenylspiro[isobenzofuran-1,4'-pyran] hydrochloride, m.p. 234.5° - 235.5°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03957828 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-8a31128ec994482a842503ae49020aa6 |
| Source note | uspto-grants-1976_05 |