Methylparaben → HCID 53868590, compound
Reaction equation
[CH3:1][O:2][C:3](=[O:11])[C:4]1[CH:9]=[CH:8][C:7]([OH:10])=[CH:6][CH:5]=1.Br[CH:13]([CH2:15][CH2:16][CH:17]([CH3:21])[CH:18]([CH3:20])[CH3:19])[CH3:14]>>[CH3:1][O:2][C:3](=[O:11])[C:4]1[CH:9]=[CH:8][C:7]([O:10][CH:13]([CH3:14])[CH2:15][CH2:16][CH:17]([CH3:21])[CH:18]([CH3:20])[CH3:19])=[CH:6][CH:5]=1Participants
3
Procedure
By utilizing the procedure of Example 19, by reacting p-hydroxybenzoic acid methyl ester with 2-bromo-5,6-dimethyl heptane, there is obtained p-[(1,4,5-trimethylhexyl)oxy]benzoic acid methyl ester; nD25 = 1.4938.
Sources & evidence
- ORD record
- ord-5245718f64624de1b4bc587569d795c5
- Source dataset
- uspto-grants-1976_05
- Patent number
- US03957833
Reaction notes
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