HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 21489638, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Ethanol, 2-(dodecylthio)- | HCID 73835 | — |
| Reactant | Cyclopropanecarbonyl chloride | HCID 77637 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 21489638 | HCID 21489638 | — |
Reaction Steps
To a mixture of 2.0 g. 2-hydroxyethyl dodecyl sulfide, 60 ml. anhydrous ether and 1.27 g. cyclopropyl carboxylic acid chloride at 0° is added 1.3 ml. pyridine. The mixture is allowed to warm to room temperature and is stirred for three days. The product is isolated using the procedure of Example 3 to yield 3-thiapentadecyl cyclopropanecarboxylate, boiling point 131°-137° (0.03 mm.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03957849 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-370644912f2b4b8d97f756b00b6f8e1b |
| Source note | uspto-grants-1976_05 |