HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → 2-[(4-Chlorophenyl)sulfanyl]ethyl cyclopropanecarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Cyclopropanecarbonyl chloride | HCID 77637 | — |
| Reactant | 2-(p-Chlorophenylthio)ethanol | HCID 83487 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-[(4-Chlorophenyl)sulfanyl]ethyl cyclopropanecarboxylate | HCID 21489645 | — |
Reaction Steps
To a mixture of 1.88 g. 2-(4-chlorophenylthio)ethanol and 1.35 g. cyclopropylcarboxylic acid chloride in 50 ml. ether is added 2 equivalents pyridine. The reaction mixture is stirred overnight at room temperature and worked up as in Example 5 to yield 2-(4-chlorophenylthio)ethyl cyclopropanecarboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03957849 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-de40b994676a4b5f8e160d836ae9d74f |
| Source note | uspto-grants-1976_05 |