HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → Perilla alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Perillyl acetate | HCID 61780 | — |
| Product | Perilla alcohol | HCID 369312 | 97.7% |
Reaction Steps
Perillyl acetate (196 g.) derived from either of the examples mentioned and 30% aqueous sodium hydroxide (60 g.) were refluxed gently with stirring for 4 hours. The oil layer was separated and distilled under reduced pressure to give perillyl alcohol (150 g.) b.P. 80°/0.7 mm., αD20 + 102.5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03957856 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-39ae34768f2747dca013ecfce2e00257 |
| Source note | uspto-grants-1976_05 |