HRID1076867

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID4599837

Carbamimidoyl-acetic acid ethyl ester

C5H10N2O2

HCID11084437

Ethyl 3-formylbenzoate

C10H10O3

PRODUCTS

生成物

结构：CCOC(=O)C1=C(N)NC(N)=C(C(=O)OCC)C1c1cccc(C(=O)OCC)c1

HCID70631688

未命名化合物

收率 32%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

2 次

PROCEDURE

实验过程

Upon boiling a solution of 8.9 g 3-carbethoxybenzaldehyde and 13.0 g amidinoacetic acid ethyl ester in 100 ml ethanol for 2 hours, 2,6-diamino-4-(3-carbethoxyphenyl)-1,4-dihydropyridine-3,5-dicarboxylic acid diethyl ester of m.p. 191°C (ethanol) is obtained. Yield: 32% of theory.

WORKUP

后处理

customfor 2 hours