反应详情

A homogeneous clear solution is prepared by adding 3 moles of acetone to 1 mole of octene (1,2) oxide at room temperature. After adding 50 grams of 5% aqueous sulfuric acid to the solution, the acetone is evaporated off and the resulting solution is neutralized by adding an aqueous sodium hydroxide. The neutralized solution is extracted with pet ether and the extract dried over anhydrous magnesium sulfate. The pet ether is stripped off and 1,2-octanediol is obtained by distilling under vacuo, b.p. 103°-105°C/0.2 mm.

1. customA homogeneous clear solution is prepared
2. customthe acetone is evaporated off
3. additionby adding an aqueous sodium hydroxide
4. extractionThe neutralized solution is extracted with pet ether
5. dry with materialthe extract dried over anhydrous magnesium sulfate