Acetone → HCID 22484390, compound

Participants

Reaction Steps

In 50 volume parts of water are dissolved 19.0 parts of TRH. H2O and 7.5 parts of L-tartaric acid, followed by the addition of 700 volume parts of acetone. The resultant oil is rubbed with a glass rod and the crystals formed are recovered by filtration, washed with hot ethanol and dried under reduced pressure. The described procedure yields 24.5 parts of TRH tartrate-water as crystals melting at 127°C-129°C. [α]D25 =-49.45° (c=1.0 in water)

Provenance & Evidence