HuagongsheHuagongshe Chemistry Print Report · For research reference only
Maleic Acid → HCID 68138529, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Maleic Acid | HCID 444266 | — |
| Reactant | HCID 68138530 | HCID 68138530 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 68138529 | HCID 68138529 | — |
Reaction Steps
A solution of 3.3 g. of 6-methyl-8-phenoxymethylergoline in 50 ml. of diethyl ether was stirred while a solution of 0.58 g. of maleic acid in 10 ml. of diethyl ether was added in one portion. After stirring for about 1 hour, the crystalline 6-methyl-8-phenoxymethylergoline maleate salt was collected by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03959288 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-f5609e9a2f14459285126760d73ede60 |
| Source note | uspto-grants-1976_05 |