HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dibromobutane → 2-(6-bromohexyl)-1H-benz[de]isoquinoline-1,3(2H)-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dibromobutane | HCID 8056 | — |
| Reactant | 1,6-Dibromohexane | HCID 12368 | — |
| Reactant | N-[1-[4-(1,3-dihydro-1,3-dioxo-2H-benz[de]isoquinolin-2-yl)butyl]-4-piperidinyl]-N-phenylpropanamide, hydrochloride | HCID 131710247 | — |
| Product | 2-(6-bromohexyl)-1H-benz[de]isoquinoline-1,3(2H)-dione | HCID 20364507 | — |
Reaction Steps
Following the procedure of part (a) of example 31 but substituting 1,6-dibromohexane for the 1,4-dibromobutane, one obtains 2-(6-bromohexyl)-1H-benz[de]isoquinoline-1,3(2H)-dione; m.p. 95°-96°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03959286 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-9295c8121a634e6394e96ddfe9169ed1 |
| Source note | uspto-grants-1976_05 |