Hydrochloric Acid → HCID 86733472, compound

HRID 1077014Notes

Reaction equation

[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][C:8]([S:10][CH2:11][C:12](=[O:34])[C@@H:13]2[C@:30]3([CH3:31])[C@H:16]([C@H:17]4[C@H:27]([C:28](=[O:32])[CH2:29]3)[C@:25]3([CH3:26])[C@H:20]([CH2:21][C@H:22]([OH:33])[CH:23]=[CH:24]3)[CH2:19][CH2:18]4)[CH2:15][CH2:14]2)=[O:9])[CH2:3][CH2:2]1.O.[ClH:36]>>[ClH:36].[O:1]1[CH2:2][CH2:3][N:4]([CH2:7][C:8]([S:10][CH2:11][C:12](=[O:34])[C@@H:13]2[C@:30]3([CH3:31])[C@H:16]([C@H:17]4[C@H:27]([C:28](=[O:32])[CH2:29]3)[C@:25]3([CH3:26])[C@H:20]([CH2:21][C@H:22]([OH:33])[CH:23]=[CH:24]3)[CH2:19][CH2:18]4)[CH2:15][CH2:14]2)=[O:9])[CH2:5][CH2:6]1

Participants

Reactant 3

HCID 313Hydrochloric Acid

HCID 962Water

HCID 22790343HCID 22790343, compound

Product 1

HCID 86733472HCID 86733472, compound

Procedure

21-Morpholinoacetylthio-3α-hydroxy-5α-pregn-1-ene-11,20-dione (122 mg., 0.25 mmole) was dissolved in 0.1 M hydrochloric acid (2.5 ml.) and the resulting clear solution was made up to 12 ml. by the addition of distilled water to give a 1% aqueous solution of the title compound.

Sources & evidence

ORD record: ord-4ca9b37e5b394fac99e36cd1ec5b6af9
Source dataset: uspto-grants-1976_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03959260

Reaction notes

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