Trimethylamine → Trimethylamine

HRID 1077096Notes

Reaction equation

HRID 1077096 reaction equation
[CH2:1]=[CH:2][CH:3]([Cl:6])[CH2:4][Cl:5].[CH3:7][N:8]([CH3:10])[CH3:9].C[P:12](C)C>>[CH3:7][N:8]([CH3:10])[CH3:9].[PH3:12].[CH2:1]=[CH:2][CH:3]([Cl:6])[CH2:4][Cl:5]

Participants

6

Reactant 3

HCID 1146TrimethylamineHCID 129713,4-Dichloro-1-buteneHCID 68983Trimethylphosphine

Product 3

HCID 1146TrimethylamineHCID 129713,4-Dichloro-1-buteneHCID 24404Phosphine

Procedure

A process for producing 4-chloro-2-butenyl trimethyl ammonium or phosphonium chloride which comprises reacting 3,4-dichlorobutene-1 with trimethyl amine or trimethyl phosphine, in a molar ratio of trimethyl amine or phosphine to 3,4-dichlorobutene-1 of about 2:1 to about 0.5:1 in a solvent at a temperature of from about 0°C to about 50°C, for a period of time sufficient to yield the desired product.

Sources & evidence

ORD record
ord-2e02f04d13d6496faffbfb2bb416fd14
Source dataset
uspto-grants-1976_05
Patent number
US03959376

Reaction notes

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