反应详情

A solution of 152 g. of 2-bromobenzhydrol, 1 liter of methanol, and 45 ml. of conc. hydrochloric acid is heated under reflux for 24 hours, cooled, stirred with 100 g. of potassium carbonate, filtered, and distilled to provide 2-bromobenzhydryl methyl ether, b.p. 126°-128° (0.7 mm.).

1. temperatureunder reflux for 24 hours
2. temperaturecooled
3. filtrationof potassium carbonate, filtered
4. distillationdistilled