HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-N,N-dimethylethylamine → HCID 12361782, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-N,N-dimethylethylamine | HCID 7901 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Cyclindole | HCID 36082 | — |
| Reactant | Tetrafluoro-m-phenylenediamine dihydrochloride | HCID 149026 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 12361782 | HCID 12361782 | — |
Reaction Steps
Following the procedure given in Example 11 and using 6.7 g. of 3-(dimethylamino)-1,2,3,4-tetrahydrocarbazole, 1.35 g. of sodium hydride and 3.37 g. of dimethylaminoethyl chloride in 75 ml. of dimethylformamide there was otained 5.6 g. of 3-(dimethylaino)-9-[2-(dimethylamino)ethyl]-1,2,3,4-tetrahydrocarbazole in the form of its dihydrochloride salt which melted at 269°-270°C. (dec.) (corr.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03959309 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-47fb61e34077483ea3f49f1817ea15e5 |
| Source note | uspto-grants-1976_05 |