Hydrochloric Acid → HCID 12361800, compound

HRID 1077349Notes

Reaction equation

HRID 1077349 reaction equation
Cl.Cl.[CH3:3][N:4]([CH3:19])[CH:5]1[CH2:17][C:16]2[C:15]3[C:10](=[C:11]([F:18])[CH:12]=[CH:13][CH:14]=3)[NH:9][C:8]=2[CH2:7][CH2:6]1>CCOCC>[CH3:3][N:4]([CH3:19])[CH:5]1[CH2:17][C:16]2[C:15]3[C:10](=[C:11]([F:18])[CH:12]=[CH:13][CH:14]=3)[NH:9][C:8]=2[CH2:7][CH2:6]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 12361801HCID 12361801, compound

Product 1

HCID 12361800HCID 12361800, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

Following the procedure given in Example 3 and using 7.8 g. of 4-dimethylaminocyclohexanone and 9 g. of 2-fluorophenylhydrazine hydrochloride there was obtained, after treatment of the free base in ether with ethereal hydrogen chloride, 6.5 g. of 3-(dimethylamino)-8-fluoro-1,2,3,4-tetrahydrocarbazole hydrochloride, m.p. 298°-302°C.

Sources & evidence

ORD record
ord-ab9fa0907bd6466895cc6781e1346fe5
Source dataset
uspto-grants-1976_05
Patent number
US03959309

Reaction notes

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