HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Mercaptoethanol → 2-(beta-Hydroxyethylthio)-4-Acetylaminonitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Mercaptoethanol | HCID 1567 | — |
| Reactant | n-(3-chloro-4-nitrophenyl)acetamide | HCID 236820 | — |
| Product | 2-(beta-Hydroxyethylthio)-4-Acetylaminonitrobenzene | HCID 19431122 | — |
Reaction Steps
Starting with 42.9 g (0.2 mol) of 2-chloro-4-acetylaminonitrobenzene and 23.4 g (0.3 mol) of 2-mercaptoethanol, pale yellow crystals (46.6 g) of the expected compound are obtained, the melting point of which is 174° C. (recrystallized from 96° ethanol) and the elemental analysis of which, calculated for C10H12N2O4S.1/2CH3CH2OH, is:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05542952 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-5b90eb4aadb64a57a5463eaf147895a4 |
| Source note | uspto-grants-1996_08 |