HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19431302, compound → HCID 19431320, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19431302 | HCID 19431302 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19431320 | HCID 19431320 | — |
Reaction Steps
A solution of 5,6-dimethoxy-3-(4-methoxyphenyl)indene (1.5 g, 5.32 mmol) in 60 ml of ethanol is hydrogenated in an autoclave in the presence of palladium on carbon (10%, 25 mg) under 5 bars of hydrogen for 1.5 h. After filtration of the catalyst, the evaporation of the solvent gives an oil which gradually solidifies (1.5 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05543298 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-e48a5b729d5640b395a7660d964690e0 |
| Source note | uspto-grants-1996_08 |