HRID1077493

反应详情

EQUATION

反应方程式

HRID 1077493 的结构方程式

PROCEDURE

实验过程

Substantially the same procedure as in Reference Example 70 was repeated using 1.0 g (5.88 mmol) of 5,6-diamino-1,3-dimethyluracil and 1.44 g (6.45 mmol) of 2,4-dimethoxy-3-methylcinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane to give 581 mg (yield 28%) of Compound 103 as pale yellow needles.

WORKUP

后处理

  1. customThen, the resultant crude crystals were recrystallized from dioxane