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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1077493Erstellt: 26. Oktober 2026

5,6-Diamino-1,3-dimethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,4-dimethoxy-3-methylphenyl)ethenyl)-1,3-dimethyl-, (E)-

https://huagongshe.com/reaction/1077493

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt5,6-Diamino-1,3-dimethyluracilHCID 79501—
Edukt2,4-Dimethoxy-3-methylcinnamic acidHCID 53401577—
Produkt1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,4-dimethoxy-3-methylphenyl)ethenyl)-1,3-dimethyl-, (E)-HCID 644887028%

Reaktionsschritte

Substantially the same procedure as in Reference Example 70 was repeated using 1.0 g (5.88 mmol) of 5,6-diamino-1,3-dimethyluracil and 1.44 g (6.45 mmol) of 2,4-dimethoxy-3-methylcinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane to give 581 mg (yield 28%) of Compound 103 as pale yellow needles.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05543415
Quelldatensatzuspto-grants-1996_08
ORD IDord-24ee5497ba804854abec01e656a879ba
Quellennotizuspto-grants-1996_08