Hydrogen Peroxide → HCID 19431996, compound

HRID 1077585Notes

Reaction equation

HRID 1077585 reaction equation
[CH3:1][CH:2]1[C:6](=[O:7])[CH:5]([CH3:8])[CH2:4][S:3]1.OO.[CH3:11][OH:12]>>[CH3:1][C:2]1([O:12][CH3:11])[C:6](=[O:7])[CH:5]([CH3:8])[CH2:4][S:3]1

Participants

4

Reactant 3

HCID 784Hydrogen PeroxideHCID 887MethanolHCID 5299612,4-dimethylthiolan-3-one

Product 1

HCID 19431996HCID 19431996, compound

Procedure

To a solution of 411 g (3.16 mol) of 2,4-dimethyl-tetrahydro-thiophen-3-one in 3000 ml of methanol are added dropwise, at an internal temperature of 63°-65° and over a period of one hour, 256.4 g (2.70 mol) of 35.8% hydrogen peroxide.

Sources & evidence

ORD record
ord-6a3ed74cf78f4f598469ee0e76a8877e
Source dataset
uspto-grants-1996_08
Patent number
US05543531

Reaction notes

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