HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalic Anhydride → HCID 19698913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalic Anhydride | HCID 6811 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 19698939 | HCID 19698939 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19698913 | HCID 19698913 | — |
Reaction Steps
8-Bromo-2-methylaminooctane is treated with phthalic anhydride in toluene in the presence of triethylamine under reflux. The solvent is removed in vacuo. The residue, when triturated with water, acidified with hydrochloric acid and crystallized from alcohol will yield N-(8-bromo-2-methyloctyl)phthalimide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05543507 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-cc22abfff38d4a1494e483a29d71a742 |
| Source note | uspto-grants-1996_08 |