HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10704523, compound → 1-(4-trifluoromethylphenyl)imidazolidin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10704523 | HCID 10704523 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 1-(4-trifluoromethylphenyl)imidazolidin-2-one | HCID 10680951 | 81.9% |
Reaction Steps
1-(4-Trifluoromethylphenyl)-2(1H,3H)-imidazolone (1.15 g) was dissolved in 20 ml of acetic acid. 10% Palladium-carbon (0.3 g) was added thereto and the mixture was stirred under a hydrogen stream for six hours. The catalyst was filtered off, the solvent was distilled off and the residue was recrystallized from ethyl acetate-diisopropyl ether to give 0.95 g of 1-(4-trifluoromethylphenyl)-2-imidazolidinone as colorless prisms.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05545652 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-bfb5d0481829473cb2ea3ef28bac0159 |
| Source note | uspto-grants-1996_08 |