HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20086705, compound → HCID 178440055, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20086705 | HCID 20086705 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178440055 | HCID 178440055 | 64.6% |
Reaction Steps
A solution of 0.05 g N-phenyl-2-(aminocarbonyl)ethyl 4-ethyl-2-propyl-1-[[2'-(N-triphenylmethyl(tetrazol-5-yl) )biphenyl-4-yl]methyl]imidazole-5-carboxylate in 2.5 mL MeOH was refluxed overnight under N2. The reaction was evaporated to dryness and the residue immediately purified by flash chromatography with 0-5% MeOH/CHCl3 gradient to give 0.0226 g of pure product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05545651 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-3bea80d1fe2c45809953e632a64d9384 |
| Source note | uspto-grants-1996_08 |