HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1,1,3,3,3-Hexachloro-2,2-difluoropropane → 1,1,3,3-Tetrachloro-2,2-difluoropropane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1,1,3,3,3-Hexachloro-2,2-difluoropropane | HCID 76650 | — |
| Reactant | 1,1,3,3,3-Pentachloro-2,2-difluoropropane | HCID 150250 | — |
| Product | 1,1,3,3-Tetrachloro-2,2-difluoropropane | HCID 15084881 | — |
Reaction Steps
The reaction was conducted and the product was analyzed in the same manner as in Example 1-1 except that 34 g (0.12 mol) of CCl3CF2CCl3 was used. As a result, it was found that the conversion was 84%, and CHCl2CF2CCl3 formed at a selectivity of 46% and CHCl2CF2CHCl2 formed at a selectivity of 44%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05545777 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-8b3209dbf6a44e4b8fd1bb65bfb5f113 |
| Source note | uspto-grants-1996_08 |