HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-4-(p-fluorophenyl)-1-silacyclohexane → HCID 178455750, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-4-(p-fluorophenyl)-1-silacyclohexane | HCID 123866780 | — |
| Reactant | 1-Chloro-4-(3,4-difluorophenyl)-1-silacyclohexane | HCID 131719128 | — |
| Reactant | HCID 178445618 | HCID 178445618 | — |
| Reactant | HCID 178455748 | HCID 178455748 | — |
| Product | HCID 178455750 | HCID 178455750 | — |
Reaction Steps
The preparation was conducted in the same manner as in Example 18, except that 22.8 g (100 mmol) of 1-chloro-4-(p-fluorophenyl)-1-silacyclohexane and 2-(trans-4-ethylcyclohexyl) ethylmagnesium bromide were used instead of 24.6 g (100 mmol) of 1-chloro-4-(3,4-difluorophenyl)-1-silacyclohexane and 2-(trans-4-n-butylcyclohexyl)ethylmagnesium bromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05547606 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-f6debdbb0fdd457cb3a055f37d5450ee |
| Source note | uspto-grants-1996_08 |