HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178444430, compound → HCID 178444429, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178444430 | HCID 178444430 | — |
| Reactant | HCID 178505835 | HCID 178505835 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178444429 | HCID 178444429 | — |
Reaction Steps
A 15 ml THF solution of 1.0M 3,4-difluorophenylmagnesium bromide (15 mmol) was dripped into a mixed solution of 2.5 g (7.9 mmol) of 1-chloro-4-(2-(trans-4-n-pentylcyclohexyl) ethyl)-1-silacyclohexane and 50 ml of THF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05547606 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-d8f4139ed86d4da68763b0d4de5629fe |
| Source note | uspto-grants-1996_08 |