HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19428551, compound → HCID 67769887, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19428551 | HCID 19428551 | — |
| Reactant | HCID 57078569 | HCID 57078569 | — |
| Product | HCID 67769887 | HCID 67769887 | 77.5% |
Reaction Steps
The reaction of 16α-methyl-21-(4-nitrobenzenesulfonyloxy)pregna-1,4,9(11)-triene-3,20-dione with 2,4-bis(4,4-ethylenedioxy-1-piperidinyl)-6-(1-piperazinyl)pyrimidine as described in Example 5 leads to the title compound in a yield of 77.5%, m.p.:156°-174° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05547949 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-890c77f5655e4314a1bd03d303e46004 |
| Source note | uspto-grants-1996_08 |